Using the FDCS freeze drying cryo stage and light microscopy techniques such as phase contrast and polarised light, it is now possible to quickly and accurately determine collapse and eutectic temperature and intricately investigate the freeze dried structure of complex samples.
Both stage pressure and temperature can be accurately controlled and programmed to simulate industrial procedures and determine ideal drying parameters.
With a temperature range down to < -195°C, ultra low temperature eutectics can be investigated with the FDCS system.
Chamber pressure is monitored by a Pirani gauge mounted directly on the stage which is able to hold perfectly uniform vacuum even when the XY manipulators are used to follow the drying front moving across the sample.
The FDCS196 is available with either NEXUS software for computer control and recording, or a LinkPad touch screen for stand-alone control.
Temperature range < -195°C to 125°C
Up to 150°C/min heating
Temperature stability <0.1°C
15mm XY sample manipulation
Sample area 22mm diameter
Maximum vacuum tested to 10-3mbar (tested onsite under full vacuum load)
Clamps directly to the microscope substage for stability
100 Ohm platinum resistor sensor
Light aperture 1.3mm diameter
Silver heating block for high thermal conductivity
Direct injection of the coolant into the silver block
Single ultra thin lid window 0.5mm
Objective lens working distance 4.8mm
Condenser lens minimum working distance 12.5mm
Range of condenser extension lenses available
Can be used with all microscope techniques
Suitable for confocal, Laser Raman, IR and X-ray
Stage body size 135mm x 92mm x 21.7mm